Green Propylhexedrine Synthesis

Green Propylhexedrine Synthesis is when you condense Cyclohexyl-2-Propanone with Methylamine in ethanol water and get Cyclohexyl-2-Propanone Methylimine intermediate. Then you add Carbonic Acid, Formic Acid, Ammonium Carbonate, Ammonium Formate, Potassium Formate, and Dry Ice (Solid CO2). The point is making an inert atmosphere of CO2 gas. Then use Aluminum Galinstan amalgam plus 500mg Palladium on Carbon or Aluminum Palladium Galinstan amalgam (25mg to 50mg Palladium) to reduce the double bond of Cyclohexyl-2-Propanone Methylimine to Propylhexedrine (Cyclohexylmethylaminopropane). Then filter through a Buchner Funnel careful not to pour off the Palladium Galinstan, add dry ethanol, pour off and filter, then put in a beaker and dry the contents of the Buchner Funnel with anhydrous MgSO4. Then filter through a Buchner Funnel again and collect it and bubble HCl gas through it to get Propylhexedrine HCl powder. Use an Acetone wash to get rid of excess HCl. Recrystallize from dry Isopropyl Alcohol to get Propylhexedrine HCl crystals.

I synthesized Propylhexedrine from Cyclohexyl-2-Propanone Methylimine using Ammonium Carbonate, Ammonium Formate, and either Aluminum Galinstan amalgam and 500mg Palladium on Carbon or Aluminum Palladium Galinstan amalgam. This is Green Propylhexedrine Synthesis. Aluminum Galinstan amalgam plus Palladium on Carbon or Aluminum Palladium Galinstan amalgam is a Green alternative to Aluminum Mercury amalgam.

Green Propylhexedrine Synthesis by HawaiianPunch1 July 5, 2024